Preparation of Ni-cBN composites by spark plasma sintering

Fabrication and Characteristics of 8YSZ/Ni functionally Graded Materials by Applying Spark Plasma Sintering Procedure (RESEARCH NOTE)

Functionally graded materials (FGM) in the form of layered structure consisting of yttria stabilized zirconia (8 mol% Y2O3) and nickel were fabricated by spark plasma sintering procedure. The relative density, linear shrinkage and Vickers hardness of each layer of graded materials were measured. The microstructure and the composition of these components were studied. The results obtained show t...

Characterization of Multiwalled Carbon Nanotube-Reinforced Hydroxyapatite Composites Consolidated by Spark Plasma Sintering

Pure HA and 1, 3, 5, and 10 vol% multiwalled carbon nanotube- (MWNT-) reinforced hydroxyapatite (HA) were consolidated using a spark plasma sintering (SPS) technique. The relative density of pure HA increased with increasing sintering temperature, but that of the MWNT/HA composite reached almost full density at 900°C, and then decreased with further increases in sintering temperature. The relat...

Binary Alkali-Metal Silicon Clathrates by Spark Plasma Sintering: Preparation and Characterization

The binary intermetallic clathrates K8-xSi46 (x = 0.4; 1.2), Rb6.2Si46, Rb11.5Si136 and Cs7.8Si136 were prepared from M₄Si₄ (M = K, Rb, Cs) precursors by spark-plasma route (SPS) and structurally characterized by Rietveld refinement of PXRD data. The clathrate-II phase Rb11.5Si136 was synthesized for the first time. Partial crystallographic site occupancy of the alkali metals, particularly for ...

Optically transparent ceramics by spark plasma sintering of oxide nanoparticles

Fabrication of Nanostructured Cu matrix Nanocomposites by High Energy Mechanical Milling and Spark Plasma Sintering

Spark plasma sintering (SPS) is a sintering process that is capable of sintering hard worked powders in short times. This technique was used to fabricate bulk Cu and Cu-SiC nanocomposites. Pure Cu and mixed powders of Cu including 4 vol% of SiC nanoparticles were mechanically alloyed for 25 h and sintered at 750˚C under vacuum condition by SPS method. Microstructures of the materials were chara...